This standard is issued under the fixed designation D ; the number 1 This test method is under the jurisdiction of ASTM Committee D on Plastics. ASTM D Standard Test Method for Transition Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential. ASTM D – MELTING POINT BY DSC TESTING SERVICES – ASTM D is a method of measuring transition temperatures by Differential Scanning.

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The sample compartment is where an encapsulated sample of about 10 to 15 milligrams is placed for testing.

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The sample is heated at a controlled rate and a plot of heat flow versus temperature is produced. Material testing you can trust since Link to Active This link will always route to the current Active version of the standard. Engage with an expert today.

Using a DSC differential scanning calorimeter the following are commonly determined: Most commonly used for detecting glass transition temperature and other thermal properties, differential scanning calorimetry is one of the most efficient and cost-effective polymer test methods available.

Certain equipment allows the temperature range to be extended. Our deliverable is certainty – high quality data, test reports and certifications that you can rely on when making decisions about your materials and components.


We have no amendments or corrections for this standard. The ISO procedures provide additional information not supplied by this test method.

Differential Scanning Calorimeter ASTM D3418, ASTM E1356, ISO 11357

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True heats of fusion are to be determined in conjunction with structure investigation, and frequently, specialized crystallization techniques are needed. The signal from the DSC is usually plotted with temperature on the X-axis and heat energy on the Y-axis. Contact an expert today to let us know how we can make your next project a success.

Differential Scanning Calorimetry Analysis – DSC – ASTM D, ASTM D | Element

The reference compartment contains an empty aluminum pan and cover equivalent to those used to encapsulate a test sample. Send us a request Need help or have a question? Auditing Consulting Sourcing Training. Change in specific heat capacity, heat flow and temperature values adtm determined for these transitions.

Need more than one copy? Doing business with one of our laboratories enables our clients’ access to our global platform of expertise, capacity and capabilities. Certain equipment allows the temperature range to be extended. If the sample under test requires more energy compared to the reference, it is indicated as an endotherm.

The energy required to heat the sample is compared to an inert reference material at the same temperature.

Differential Scanning Calorimeter ASTM D, ASTM E, ISO

To perform DSC testing, a small amount of material is heated at a predetermined rate. This standard is not included in any packages. Historical Version s – view previous versions of standard. Validating the specifications, value and safety of your raw materials, products and assets. Both pans are heated at the same temperature ramp rate and the energy required to keep each one heating is continuously measured.


Element offers a variety of methods for determining glass transition temperature and other important polymeric characteristics. 3d418 Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.

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As the voice of the U. Weak glass transitions such as in polyethylene and polypropylene are usually not strong enough to detect. By using our website you consent to all cookies in accordance with our Cookie Policy. Phenolic materials typically give off water as a by product of curing which boils and shows a downward endothermic peak in the same range as the curing exothermic peak so they cancel each other out.

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Differential Scanning Calorimetry (DSC) Analysis

It is also used to characterize materials for their thermal performance. Already Subscribed to this document.

Active view current version of standard Translated Standard: Enabling you to identify and mitigate the intrinsic risk in your operations, supply chains and business processes. DSC testing has been used for decades as a way to predict the behaviors of polymeric materials under different thermal conditions.

Measures the temperature and energy of thermal transitions such as melting point, glass transition, and curing reactions. Need help or have a question?

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